DONATH, K. S.; DONATH, Katia Shimabukuro.
Abstract:
Metallic porous coatings have been used on hip orthopedic prostheses to
promote ingrowth of bone into the porous coating prostheses. Among different
materials used to manufacture hip prostheses and coatings are titanium
materials. Mostly used and available are commercially pure titanium and Ti-6Al4V
alloy. Titanium and its alloys are allotrope. Its characteristics are influenced
by two principal factors: chemical composition and microstructure. Thickness,
porosity, pore size e interconnectivity between pores and coating are important
for the bone growth and prosthesis fixation. Different mechanism of hip
prosthesis failures in result of the coating placed on the prosthesis have been
reported in the literature. In this thesis various technical standards for Titanium
commercially pure and Ti-6Al-4V were identified. They are related to the
material, the forging and metallic powders for coatings, Furthermore, evaluation
methods for coating and industry guidelines, some with acceptance criteria,
some without, were found. Within the standard ABNT NBR 15628-4
inconsistencies regarding the required microstructures were found. Technical
standards were compared and linked to data from the literature. Critical points
related to porous metallic coating, production methods, its effects on Ti-6Al-4V
substrate and characteristics of porous coatings. 8 in Brazil commercially
available products were evaluated considering their registration at ANVISA and
analysis of their coatings in a lab. The chemical composition of the substrate
was determined by optical emission spectroscopy. Optical microscopy was
used to evaluate the microstructure of the substrate and for stereological
analysis of the coating. Chemical composition analyses of the substrate pointed
2 components made of Titanium commercially pure and 6 made of Ti-6Al-4V.
One sample had results of substrate according Ti-6Al-4V alloy besides
registration information at ANVISA described substrate made of Ti commercially
pure. Regarding the microstructural analysis of the substrate, the majority of
problems occurred with products made by sintering and by foreign producers.
50% of products made by Ti-6Al-4V presented microstructures with continuous
alpha phase on the beta grain boundaries. Therefore it can be concluded that
they were processed at temperatures higher than beta transus temperatures.
Analyzing the thickness of the coating, all samples from foreign producers had a
bigger thickness than any national product. No national product had a thickness
bigger than 500µm. Therefore it is possible to conclude that the microstructure
was affected by the thermic processes and that those need better controls,
regulation and surveillance in order to supply more secure and effective
products.